https://doi.org/10.1021/ac951209b

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College of Arts and Sciences Publications and Scholarship

ORCID

https://orcid.org/0000-0003-2365-1175

Abstract

A new method of ohmic potential drop correction for use with potential step and sweep voltammetric methods is described. The method, iterative correction of the applied potential (ICAP), essentially replaces an electronic positive feedback correction with a digital positive feedback correction. This paper will present one form of the ICAP procedure, in which voltammetric current data acquired by a high-speed digital oscilloscope are used to iteratively generate a compensating potential waveform that is then synthesized by an arbitrary waveform generator. The ICAP method is advantageous for high-speed measurements, since many of the difficulties caused by electronic positive feedback compensation are eliminated.

Publisher

Analytical Chemistry

First Page

1971

Last Page

1876

Publication Date

1996

College

College of Arts and Sciences

Department

Department of Chemistry

Keywords

voltammetry, cyclic voltammetry, electrochemistry, ohmic drop

Disciplines

Analytical Chemistry | Physical Chemistry

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