Theses and Dissertations
Issuing Body
Mississippi State University
Advisor
Sullivan, Rani Warsi
Committee Member
Pittman, Charles U., Jr.
Committee Member
Toghiani, Hossein
Committee Member
DuBien, Janice
Committee Member
Lacy, Thomas E.
Date of Degree
5-11-2013
Document Type
Graduate Thesis - Open Access
Major
Aerospace Engineering
Degree Name
Master of Science
College
James Worth Bagley College of Engineering
Department
Department of Aerospace Engineering
Abstract
The effects of vapor-grown carbon nanofiber (VGCNF) weight fraction, applied stress, and temperature on the viscoelastic responses (creep strain, creep rate, and creep compliance) of VGCNF/vinyl ester (VE) nanocomposites were studied using a central composite design (CCD). The nanocomposite test articles were fabricated by high shear mixing, casting, curing, and post-curing in an open face mold under a nitrogen environment. Short-term creep/creep recovery experiments were conducted at prescribed combinations of temperatures (23.8 – 69.2 C), applied stresses (30.2 – 49.8 MPa), and VGCNF weight fractions (0.00 – 1.00 parts of VGCNF per hundred parts of resin, phr) determined from the CCD. The response surface models (RSMs) for predicting these viscoelastic responses were developed using the least squares method and an analysis of variance procedure. The response surface estimates indicate that increasing the VGCNF weight fraction decreases the creep resistance of the VGCNF/VE nanocomposites at high temperatures (46.5 – 69.2 C).
URI
https://hdl.handle.net/11668/20554
Recommended Citation
Drake, Daniel Adam, "Viscoelastic Characterization of Vapor-Grown Carbon Nanofiber/Vinyl Ester Nanocomposites using a Response Surface Methodology" (2013). Theses and Dissertations. 4964.
https://scholarsjunction.msstate.edu/td/4964